Information card for entry 4301415

Structure parameters

• Formula: C42 H84 Au2 Cl4 N6 O2 P4 Rh2
• Calculated formula: C42 H84 Au2 Cl4 N6 O2 P4 Rh2
• Title of publication: An Acyclic Dimer of Cyclodiphosphazane {tBuHN(tBuNP)2OCH2}2 Containing Alkoxo and Amido Functionalities: Synthesis, Derivatization, Bi- (PdII, RhI), and Tetranuclear (PdII, AuI, RhIAuI) Transition Metal Complexes
• Authors of publication: Maravanji S. Balakrishna; Ramalingam Venkateswaran; Joel T. Mague
• Journal of publication: Inorganic Chemistry
• Year of publication: 2009
• Journal volume: 48
• Pages of publication: 1398 - 1406
• a: 14.156 ± 0.002 Å
• b: 19.09 ± 0.003 Å
• c: 21.947 ± 0.003 Å
• α: 90°
• β: 107.241 ± 0.001°
• γ: 90°
• Cell volume: 5664.4 ± 1.4 ų
• Cell temperature: 110 ± 2 K
• Ambient diffraction temperature: 110 ± 2 K
• Number of distinct elements: 8
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0811
• Residual factor for significantly intense reflections: 0.0582
• Weighted residual factors for significantly intense reflections: 0.1195
• Weighted residual factors for all reflections included in the refinement: 0.1303
• Goodness-of-fit parameter for all reflections included in the refinement: 1.039
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Duplicate of: 4301408
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No