Information card for entry 4301478

Structure parameters

• Formula: H106 Lu2.8 Na2 O137 W22
• Calculated formula: Lu2.8 Na2 O114.5 W22
• Title of publication: 22-Isopolytungstate Fragment [H2W22O74]14-Coordinated to Lanthanide Ions
• Authors of publication: Amal H. Ismail; Michael H. Dickman; Ulrich Kortz
• Journal of publication: Inorganic Chemistry
• Year of publication: 2009
• Journal volume: 48
• Pages of publication: 1559 - 1565
• a: 12.4655 ± 0.0008 Å
• b: 12.6027 ± 0.0009 Å
• c: 19.3294 ± 0.0016 Å
• α: 72.674 ± 0.004°
• β: 74.281 ± 0.004°
• γ: 86.987 ± 0.004°
• Cell volume: 2789.1 ± 0.4 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0877
• Residual factor for significantly intense reflections: 0.0502
• Weighted residual factors for significantly intense reflections: 0.1211
• Weighted residual factors for all reflections included in the refinement: 0.1429
• Goodness-of-fit parameter for all reflections included in the refinement: 1.031
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No