Information card for entry 4301661

Structure parameters

• Formula: C36.67 H48.33 Cl5.33 F6 N3 P Ru Sb
• Calculated formula: C36.66 H48.32 Cl5.32 F6 N3 P Ru Sb
• Title of publication: Intramolecular Hydrogen-Bonded Tertiary Phosphines as 1,3,5-Triaza-7-phosphaadamantane (PTA) Analogues
• Authors of publication: Allen T. Ekubo; Mark R. J. Elsegood; Andrew J. Lake; Martin B. Smith
• Journal of publication: Inorganic Chemistry
• Year of publication: 2009
• Journal volume: 48
• Pages of publication: 2633 - 2638
• a: 12.9426 ± 0.0005 Å
• b: 14.0425 ± 0.0005 Å
• c: 14.7175 ± 0.0006 Å
• α: 65.2785 ± 0.0005°
• β: 70.5853 ± 0.0005°
• γ: 66.5392 ± 0.0005°
• Cell volume: 2184.22 ± 0.15 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 8
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0442
• Residual factor for significantly intense reflections: 0.0377
• Weighted residual factors for significantly intense reflections: 0.0991
• Weighted residual factors for all reflections included in the refinement: 0.1033
• Goodness-of-fit parameter for all reflections included in the refinement: 1.028
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No