Information card for entry 4301672

Structure parameters

• Formula: C42 H52 Cl2 O2 P4
• Calculated formula: C42 H52 Cl2 O2 P4
• Title of publication: Intramolecular Phosphine-Phosphine Donor-Acceptor Complexes
• Authors of publication: Piotr Wawrzyniak; Amy L. Fuller; Alexandra M. Z. Slawin; Petr Kilian
• Journal of publication: Inorganic Chemistry
• Year of publication: 2009
• Journal volume: 48
• Pages of publication: 2500 - 2506
• a: 27.883 ± 0.006 Å
• b: 11.919 ± 0.003 Å
• c: 26.114 ± 0.005 Å
• α: 90°
• β: 114.549 ± 0.008°
• γ: 90°
• Cell volume: 7894 ± 3 ų
• Cell temperature: 93 ± 2 K
• Ambient diffraction temperature: 93 ± 2 K
• Number of distinct elements: 5
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.1184
• Residual factor for significantly intense reflections: 0.0891
• Weighted residual factors for significantly intense reflections: 0.1816
• Weighted residual factors for all reflections included in the refinement: 0.1958
• Goodness-of-fit parameter for all reflections included in the refinement: 1.124
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No