Information card for entry 4301746

Structure parameters

• Formula: C17 H43 B2 F8 N4 Os P
• Calculated formula: C17 H43 B2 F8 N4 Os P
• Title of publication: Monocationic Trihydride and Dicationic Dihydride-Dihydrogen and Bis(dihydrogen) Osmium Complexes Containing Cyclic and Acyclic Triamine Ligands: Influence of the N-Os-N Angles on the Hydrogen-Hydrogen Interactions
• Authors of publication: Miguel Baya; Miguel A. Esteruelas; Montserrat Oliván; Enrique Oñate
• Journal of publication: Inorganic Chemistry
• Year of publication: 2009
• Journal volume: 48
• Pages of publication: 2677 - 2686
• a: 8.1936 ± 0.0014 Å
• b: 33.085 ± 0.006 Å
• c: 9.7024 ± 0.0016 Å
• α: 90°
• β: 94.868 ± 0.003°
• γ: 90°
• Cell volume: 2620.7 ± 0.8 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0572
• Residual factor for significantly intense reflections: 0.041
• Weighted residual factors for significantly intense reflections: 0.0783
• Weighted residual factors for all reflections included in the refinement: 0.0829
• Goodness-of-fit parameter for all reflections included in the refinement: 0.988
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No