Information card for entry 4301839

Structure parameters

• Chemical name: [K-(2,2,2-crypt)]6[Pb9Cd(C6H5)]*2en*tol
• Formula: C131 H250 Cd2 K6 N16 O36 Pb18
• Calculated formula: C131 H250.02 Cd2 K6 N16 O36 Pb18
• Title of publication: Coupling Reactions of Functionalized Zintl Ions [E9Cd(C6H5)]3- (E = Sn, Pb) with Tributyltinhydride: Synthesis and Isolation of {Sn9CdSn[(CH2)3CH3]3}3-
• Authors of publication: Binbin Zhou; Mark S. Denning; Thomas A. D. Chapman; Jose M. Goicoechea
• Journal of publication: Inorganic Chemistry
• Year of publication: 2009
• Journal volume: 48
• Pages of publication: 2899 - 2907
• a: 15.8896 ± 0.0001 Å
• b: 22.6342 ± 0.0001 Å
• c: 27.7421 ± 0.0002 Å
• α: 88.022 ± 0.0003°
• β: 74.916 ± 0.0002°
• γ: 89.5042 ± 0.0002°
• Cell volume: 9627.89 ± 0.1 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.066
• Residual factor for significantly intense reflections: 0.0456
• Weighted residual factors for significantly intense reflections: 0.1174
• Weighted residual factors for all reflections included in the refinement: 0.1248
• Goodness-of-fit parameter for all reflections included in the refinement: 1.025
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No