Information card for entry 4301877

Structure parameters

• Formula: C39 H21.5 F24 N4 Nd O13.25 P2
• Calculated formula: C39 H21.5 F24 N4 Nd O13.25 P2
• Title of publication: Synthesis and Coordination Properties of Trifluoromethyl Decorated Derivatives of 2,6-Bis[(diphenylphosphinoyl)methyl]pyridine N-Oxide Ligands with Lanthanide Ions
• Authors of publication: Sylvie Pailloux; Cornel Edicome Shirima; Alisha D. Ray; Eileen N. Duesler; Robert T. Paine; John R. Klaehn; Michael E. McIlwain; Benjamin P. Hay
• Journal of publication: Inorganic Chemistry
• Year of publication: 2009
• Journal volume: 48
• Pages of publication: 3104 - 3113
• a: 11.0642 ± 0.0006 Å
• b: 15.0247 ± 0.0008 Å
• c: 16.2086 ± 0.0009 Å
• α: 87.033 ± 0.003°
• β: 79.624 ± 0.002°
• γ: 75.122 ± 0.003°
• Cell volume: 2561.5 ± 0.2 ų
• Cell temperature: 225 ± 2 K
• Ambient diffraction temperature: 225 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0407
• Residual factor for significantly intense reflections: 0.0325
• Weighted residual factors for significantly intense reflections: 0.0811
• Weighted residual factors for all reflections included in the refinement: 0.0889
• Goodness-of-fit parameter for all reflections included in the refinement: 1.082
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No