Information card for entry 4301963

Structure parameters

• Formula: C17 H40 F6 N P3 Pd
• Calculated formula: C17 H40 F6 N P3 Pd
• SMILES: [Pd]12([P](CC[NH]2CC[P]1(C(C)C)C(C)C)(C(C)C)C(C)C)C.[P](F)(F)(F)(F)(F)[F-]
• Title of publication: Palladium N(CH2CH2PiPr2)2-Dialkylamides: Synthesis, Structural Characterization, and Reactivity
• Authors of publication: Alexander N. Marziale; Eberhardt Herdtweck; Jörg Eppinger; Sven Schneider
• Journal of publication: Inorganic Chemistry
• Year of publication: 2009
• Journal volume: 48
• Pages of publication: 3699 - 3709
• a: 8.6804 ± 0.0003 Å
• b: 15.6177 ± 0.0005 Å
• c: 18.5296 ± 0.0008 Å
• α: 90°
• β: 94.552 ± 0.003°
• γ: 90°
• Cell volume: 2504.1 ± 0.16 ų
• Cell temperature: 173 ± 1 K
• Ambient diffraction temperature: 173 ± 1 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0347
• Residual factor for significantly intense reflections: 0.0312
• Weighted residual factors for significantly intense reflections: 0.0769
• Weighted residual factors for all reflections included in the refinement: 0.0785
• Goodness-of-fit parameter for all reflections included in the refinement: 1.08
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No