Information card for entry 4302023

Structure parameters

• Chemical name: μ-{1,4-Bis[bis(bis(o-methoxyphenoxy)phosphino)amino] benzene-1κP;2κP';3κP";4κP'"}-μ-bis(perchlorato- 1κO;2κO;3κO;4κO)-μ-bis(perchlorato-1κO;2κO'; 3κO;4κO')tetrakis(tetrahydrofuran)tetrakis(silver(I)) Tetrahydrofuran Solvate o-Methoxyphenol Solvate
• Formula: C104 H132 Ag4 Cl4 N2 O43 P4
• Calculated formula: C104 H132 Ag4 Cl4 N2 O43 P4
• Title of publication: Group 11 Metal Chemistry of a Tetradentate Ligand, Phenylene-1,4-diaminotetra(phosphonite), p-C6H4[N{P(OC6H4OMe-o)2}2]2
• Authors of publication: Chelladurai Ganesamoorthy; Maravanji S. Balakrishna; Joel T. Mague
• Journal of publication: Inorganic Chemistry
• Year of publication: 2009
• Journal volume: 48
• Pages of publication: 3768 - 3782
• a: 13.743 ± 0.002 Å
• b: 15.53 ± 0.002 Å
• c: 16.198 ± 0.002 Å
• α: 109.135 ± 0.002°
• β: 110.464 ± 0.002°
• γ: 90.28 ± 0.002°
• Cell volume: 3032 ± 0.7 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1137
• Residual factor for significantly intense reflections: 0.0579
• Weighted residual factors for significantly intense reflections: 0.151
• Weighted residual factors for all reflections included in the refinement: 0.1686
• Goodness-of-fit parameter for all reflections included in the refinement: 0.927
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No