Information card for entry 4302178

Structure parameters

• Formula: C77 H83 B F24 Ga2 P Rh
• Calculated formula: C77 H83 B F24 Ga2 P Rh
• Title of publication: Syntheses and Crystal Structures of Ruthenium and Rhodium Olefin Complexes Containing GaCp*
• Authors of publication: Thomas Cadenbach; Christian Gemel; Timo Bollermann; Roland A. Fischer
• Journal of publication: Inorganic Chemistry
• Year of publication: 2009
• Journal volume: 48
• Pages of publication: 5021 - 5026
• a: 15.8148 ± 0.0004 Å
• b: 25.0768 ± 0.0009 Å
• c: 19.0581 ± 0.0008 Å
• α: 90°
• β: 92.723 ± 0.003°
• γ: 90°
• Cell volume: 7549.6 ± 0.5 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.1272
• Residual factor for significantly intense reflections: 0.0443
• Weighted residual factors for significantly intense reflections: 0.0481
• Weighted residual factors for all reflections included in the refinement: 0.0565
• Goodness-of-fit parameter for all reflections included in the refinement: 0.669
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No