Information card for entry 4302352

Structure parameters

• Formula: C39 H69 Li N2 O3 Zn2
• Calculated formula: C39 H69 Li N2 O3 Zn2
• Title of publication: Donor-Dictated Interlocking Co-Complexation Reactions of LiNHDipp with Dimethylzinc: Synthesis and Structures of New Methyl(amido)zincates
• Authors of publication: Clegg, William; Graham, David V.; Herd, Emma; Hevia, Eva; Kennedy, Alan R.; McCall, Matthew D.; Russo, Luca
• Journal of publication: Inorganic Chemistry
• Year of publication: 2009
• Journal volume: 48
• Journal issue: 12
• Pages of publication: 5320 - 5327
• a: 18.1783 ± 0.0001 Å
• b: 18.6099 ± 0.0002 Å
• c: 24.4975 ± 0.0002 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 8287.41 ± 0.12 ų
• Cell temperature: 123 ± 2 K
• Ambient diffraction temperature: 123 ± 2 K
• Number of distinct elements: 6
• Space group number: 61
• Hermann-Mauguin space group symbol: P b c a
• Hall space group symbol: -P 2ac 2ab
• Residual factor for all reflections: 0.0624
• Residual factor for significantly intense reflections: 0.0451
• Weighted residual factors for significantly intense reflections: 0.1094
• Weighted residual factors for all reflections included in the refinement: 0.1205
• Goodness-of-fit parameter for all reflections included in the refinement: 1.094
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Duplicate of: 4338613
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No