Information card for entry 4302476

Structure parameters

• Formula: C57.5 H65 Fe N4
• Calculated formula: C57.5 H65 Fe N4
• Title of publication: Synthesis of Bis(imino)pyridine Iron Amide and Ammonia Compounds from an N-H Transfer Agent
• Authors of publication: Amanda C. Bowman; Suzanne C. Bart; Frank W. Heinemann; Karsten Meyer; Paul J. Chirik
• Journal of publication: Inorganic Chemistry
• Year of publication: 2009
• Journal volume: 48
• Pages of publication: 5587 - 5589
• a: 11.4441 ± 0.0009 Å
• b: 13.5081 ± 0.0018 Å
• c: 16.9763 ± 0.0016 Å
• α: 71.594 ± 0.009°
• β: 76.764 ± 0.01°
• γ: 78.316 ± 0.008°
• Cell volume: 2399.7 ± 0.5 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 4
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0686
• Residual factor for significantly intense reflections: 0.045
• Weighted residual factors for significantly intense reflections: 0.1016
• Weighted residual factors for all reflections included in the refinement: 0.1128
• Goodness-of-fit parameter for all reflections included in the refinement: 1.029
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No