Information card for entry 4302491

Structure parameters

• Formula: Cu2.3 H40 Mo3 O81.33 P2 W15
• Calculated formula: Cu2.223 Mo2.94 O81.512 P2 W15.06
• Title of publication: 2D and 3D Polymeric Wells-Dawson Polyoxometelates: Synthesis, Crystal Structures, and Cyclic Voltammetry of [(M(H2O)4)x][H6-2xP2W18-nMonO62] (M = CuII, CoII, NiII)
• Authors of publication: Robila Belghiche; Ouahiba Bechiri; Mostefa Abbessi; Stéphane Golhen; Yann Le Gal; Lahcène Ouahab
• Journal of publication: Inorganic Chemistry
• Year of publication: 2009
• Journal volume: 48
• Pages of publication: 6026 - 6033
• a: 15.194 ± 0.0011 Å
• b: 15.194 ± 0.0011 Å
• c: 55.657 ± 0.001 Å
• α: 90°
• β: 90°
• γ: 120°
• Cell volume: 11127.4 ± 1.2 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 6
• Space group number: 166
• Hermann-Mauguin space group symbol: R -3 m :H
• Hall space group symbol: -R 3 2"
• Residual factor for all reflections: 0.0637
• Residual factor for significantly intense reflections: 0.0411
• Weighted residual factors for significantly intense reflections: 0.1054
• Weighted residual factors for all reflections included in the refinement: 0.1172
• Goodness-of-fit parameter for all reflections included in the refinement: 0.997
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No