Information card for entry 4302519

Structure parameters

• Common name: [Pd(pmdt)SH](Et4N)
• Formula: C15 H28 N2 Pd S3
• Calculated formula: C15 H28 N2 Pd S3
• SMILES: [Pd]12(SCc3[n]2c(ccc3)CS1)S.[N+](CC)(CC)(CC)CC
• Title of publication: Cleavage of Ni-(μ2-S)-Ni Bridges in Dinuclear Nickel(II) Dithiolate Pincer Complexes and Related Reactions
• Authors of publication: Deguang Huang; Liang Deng; Jibin Sun; R. H. Holm
• Journal of publication: Inorganic Chemistry
• Year of publication: 2009
• Journal volume: 48
• Pages of publication: 6159 - 6166
• a: 11.925 ± 0.0019 Å
• b: 12.822 ± 0.002 Å
• c: 12.559 ± 0.002 Å
• α: 90°
• β: 92.653 ± 0.002°
• γ: 90°
• Cell volume: 1918.2 ± 0.5 ų
• Cell temperature: 193 ± 2 K
• Ambient diffraction temperature: 193 ± 2 K
• Number of distinct elements: 5
• Space group number: 9
• Hermann-Mauguin space group symbol: C 1 c 1
• Hall space group symbol: C -2yc
• Residual factor for all reflections: 0.0167
• Residual factor for significantly intense reflections: 0.0166
• Weighted residual factors for significantly intense reflections: 0.0413
• Weighted residual factors for all reflections included in the refinement: 0.0414
• Goodness-of-fit parameter for all reflections included in the refinement: 1.038
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No