Information card for entry 4302522

Structure parameters

• Common name: [Ni(pdtc)OSiMe3] (Et4N)
• Formula: C18 H32 N2 Ni O3 S2 Si
• Calculated formula: C18 H32 N2 Ni O3 S2 Si
• Title of publication: Cleavage of Ni-(μ2-S)-Ni Bridges in Dinuclear Nickel(II) Dithiolate Pincer Complexes and Related Reactions
• Authors of publication: Deguang Huang; Liang Deng; Jibin Sun; R. H. Holm
• Journal of publication: Inorganic Chemistry
• Year of publication: 2009
• Journal volume: 48
• Pages of publication: 6159 - 6166
• a: 8.9067 ± 0.0005 Å
• b: 8.9772 ± 0.0005 Å
• c: 15.2903 ± 0.0009 Å
• α: 86.703 ± 0.004°
• β: 76.782 ± 0.004°
• γ: 85.129 ± 0.004°
• Cell volume: 1184.97 ± 0.12 ų
• Cell temperature: 193 ± 2 K
• Ambient diffraction temperature: 193 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0724
• Residual factor for significantly intense reflections: 0.0449
• Weighted residual factors for significantly intense reflections: 0.1102
• Weighted residual factors for all reflections included in the refinement: 0.1264
• Goodness-of-fit parameter for all reflections included in the refinement: 1.021
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No