Information card for entry 4302524

Structure parameters

• Common name: {[Ni(pdtc)]SEt[Ni(pdtc)]}(Et4N)(CH2Cl2)
• Formula: C25 H33 Cl2 N3 Ni2 O4 S5
• Calculated formula: C25 H33 Cl2 N3 Ni2 O4 S5
• Title of publication: Cleavage of Ni-(μ2-S)-Ni Bridges in Dinuclear Nickel(II) Dithiolate Pincer Complexes and Related Reactions
• Authors of publication: Deguang Huang; Liang Deng; Jibin Sun; R. H. Holm
• Journal of publication: Inorganic Chemistry
• Year of publication: 2009
• Journal volume: 48
• Pages of publication: 6159 - 6166
• a: 9.7843 ± 0.0012 Å
• b: 13.4937 ± 0.0017 Å
• c: 13.7498 ± 0.0018 Å
• α: 77.248 ± 0.002°
• β: 70.317 ± 0.002°
• γ: 79.757 ± 0.002°
• Cell volume: 1656.5 ± 0.4 ų
• Cell temperature: 193 ± 2 K
• Ambient diffraction temperature: 193 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0541
• Residual factor for significantly intense reflections: 0.0427
• Weighted residual factors for significantly intense reflections: 0.1076
• Weighted residual factors for all reflections included in the refinement: 0.1185
• Goodness-of-fit parameter for all reflections included in the refinement: 1.02
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No