Information card for entry 4302568

Structure parameters

• Formula: C65 H115 Cl0.27 Co I0.73 N5 Na O5 P3 Zr
• Calculated formula: C65 H115 Cl0.2656 Co I0.7344 N5 Na O5 P3 Zr
• Title of publication: Multielectron Redox Activity Facilitated by Metal-Metal Interactions in Early/Late Heterobimetallics: Co/Zr Complexes Supported by Phosphinoamide Ligands
• Authors of publication: Bennett P. Greenwood; Scott I. Forman; Gerard T. Rowe; Chun-Hsing Chen; Bruce M. Foxman; Christine M. Thomas
• Journal of publication: Inorganic Chemistry
• Year of publication: 2009
• Journal volume: 48
• Pages of publication: 6251 - 6260
• a: 14.761 ± 0.0009 Å
• b: 24.606 ± 0.0015 Å
• c: 19.1884 ± 0.0011 Å
• α: 90°
• β: 90.284 ± 0.003°
• γ: 90°
• Cell volume: 6969.3 ± 0.7 ų
• Cell temperature: 120 K
• Ambient diffraction temperature: 120 K
• Number of distinct elements: 10
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0499
• Residual factor for significantly intense reflections: 0.033
• Weighted residual factors for all reflections: 0.0799
• Weighted residual factors for significantly intense reflections: 0.0721
• Weighted residual factors for all reflections included in the refinement: 0.0799
• Goodness-of-fit parameter for all reflections included in the refinement: 1.0156
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No