Crystallography Open Database

Information card for entry 4302657

Preview

Coordinates	4302657.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C48 H108 Cl9 Cu8 N8 Na5 O114 Sm4
Calculated formula	C48 H108 Cl9 Cu8 N8 Na5 O114 Sm4
Title of publication	From Metalloligand to Interpenetrating Channels: Synthesis, Characterization, and Properties of a 2p-3d-4f Heterometallic Coordination Polymer {[Na5Cu8Sm4(NTA)8(ClO4)8(H2O)22].ClO4.8H2O}n
Authors of publication	Jing-xin Ma; Xiao-feng Huang; You Song; Xue-qin Song; Wei-sheng Liu
Journal of publication	Inorganic Chemistry
Year of publication	2009
Journal volume	48
Pages of publication	6326 - 6328
a	17.041 ± 0.0014 Å
b	17.041 ± 0.0014 Å
c	25.371 ± 0.002 Å
α	90°
β	90°
γ	90°
Cell volume	7367.6 ± 1 Å³
Cell temperature	293 ± 2 K
Ambient diffraction temperature	293 ± 2 K
Number of distinct elements	8
Space group number	114
Hermann-Mauguin space group symbol	P -4 21 c
Hall space group symbol	P -4 2n
Residual factor for all reflections	0.0538
Residual factor for significantly intense reflections	0.0461
Weighted residual factors for significantly intense reflections	0.1234
Weighted residual factors for all reflections included in the refinement	0.1302
Goodness-of-fit parameter for all reflections included in the refinement	1.07
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/4302657.html