Information card for entry 4302744

Structure parameters

• Formula: C47.5 H62 Br4 N8 Ni4 O15.5
• Calculated formula: C47.5 H62 Br4 N8 Ni4 O15.5
• Title of publication: Polynuclear Nickel(II) Complexes: A Magnetostructural Study of NiII4, NiII6, and NiII9 Species with Oxime Ligands
• Authors of publication: Biplab Biswas; Ulrich Pieper; Thomas Weyhermüller; Phalguni Chaudhuri
• Journal of publication: Inorganic Chemistry
• Year of publication: 2009
• Journal volume: 48
• Pages of publication: 6781 - 6793
• a: 11.7718 ± 0.0011 Å
• b: 14.5404 ± 0.0015 Å
• c: 18.589 ± 0.002 Å
• α: 72.583 ± 0.006°
• β: 79.072 ± 0.008°
• γ: 69.254 ± 0.008°
• Cell volume: 2826.6 ± 0.5 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0562
• Residual factor for significantly intense reflections: 0.0358
• Weighted residual factors for significantly intense reflections: 0.0618
• Weighted residual factors for all reflections included in the refinement: 0.0673
• Goodness-of-fit parameter for all reflections included in the refinement: 1.036
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No