Information card for entry 4302851

Structure parameters

• Formula: C42 H40 As2 F6 O6 P2 S2
• Calculated formula: C42 H40 As2 F6 O6 P2 S2
• Title of publication: Asymmetric Synthesis of Bis(tertiary arsines): Highly Stereoselective Alkylations of Diastereomers of a Chiral Phosphine-Stabilized Bis(arsenium triflate)
• Authors of publication: Michelle L. Weir; Ian A. Cade; Nathan L. Kilah; Xiangting Zhou; S. Bruce Wild
• Journal of publication: Inorganic Chemistry
• Year of publication: 2009
• Journal volume: 48
• Pages of publication: 7482 - 7490
• a: 11.5468 ± 0.0002 Å
• b: 11.2427 ± 0.0002 Å
• c: 17.0825 ± 0.0003 Å
• α: 90°
• β: 95.6724 ± 0.0012°
• γ: 90°
• Cell volume: 2206.74 ± 0.07 ų
• Cell temperature: 200 K
• Ambient diffraction temperature: 200 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0654
• Residual factor for significantly intense reflections: 0.0373
• Weighted residual factors for all reflections: 0.0571
• Weighted residual factors for significantly intense reflections: 0.0427
• Weighted residual factors for all reflections included in the refinement: 0.0427
• Goodness-of-fit parameter for all reflections included in the refinement: 1.2801
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No