Information card for entry 4302868

Structure parameters

• Formula: C12 H36 Ge2 N8 S4
• Calculated formula: C12 H36 Ge2 N8 S4
• Title of publication: Facile Access to the Hydrazone Functionalized PdGeS Cluster [{RNGe(μ-S)3}4Pd6] from the Thiogermanate Anion [{RNGe}2(μ-S)2S2]2-
• Authors of publication: Mohammad Reza Halvagar; Zohreh Hassanzadeh Fard; Lin Xiong; Stefanie Dehnen
• Journal of publication: Inorganic Chemistry
• Year of publication: 2009
• Journal volume: 48
• Pages of publication: 7373 - 7377
• a: 20.411 ± 0.005 Å
• b: 8.445 ± 0.003 Å
• c: 29.41 ± 0.005 Å
• α: 90°
• β: 110.89 ± 0.03°
• γ: 90°
• Cell volume: 4736 ± 2 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 5
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.0728
• Residual factor for significantly intense reflections: 0.0609
• Weighted residual factors for significantly intense reflections: 0.1614
• Weighted residual factors for all reflections included in the refinement: 0.1694
• Goodness-of-fit parameter for all reflections included in the refinement: 1.077
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No