Crystallography Open Database

Information card for entry 4302962

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Coordinates	4302962.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C56 H72 Ge8 O10
Calculated formula	C56 H72 Ge8 O10
Title of publication	Formation and Structures of Germanium(II) Aryloxo/Oxo Clusters
Authors of publication	Rebecca A. Green; Curtis Moore; Arnold L. Rheingold; Charles S. Weinert
Journal of publication	Inorganic Chemistry
Year of publication	2009
Journal volume	48
Pages of publication	7510 - 7512
a	12.5179 ± 0.0009 Å
b	15.381 ± 0.0011 Å
c	17.2348 ± 0.0013 Å
α	68.373 ± 0.001°
β	77.796 ± 0.001°
γ	88.38 ± 0.001°
Cell volume	3010.5 ± 0.4 Å³
Cell temperature	150 ± 2 K
Ambient diffraction temperature	150 ± 2 K
Number of distinct elements	4
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0848
Residual factor for significantly intense reflections	0.0407
Weighted residual factors for significantly intense reflections	0.0751
Weighted residual factors for all reflections included in the refinement	0.0864
Goodness-of-fit parameter for all reflections included in the refinement	1.009
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

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