Information card for entry 4303107

Structure parameters

• Formula: C20 H42 Ge Mo P2
• Calculated formula: C20 H42 Ge Mo P2
• SMILES: [Mo]123456([Ge](CC)(CC)[H]6)([P](C)(C)CC[P]1(C)C)[c]1([c]3(C)[c]4([c]2([c]51C)C)C)C
• Title of publication: Germylene and Silylene Complexes of Molybdenum via E-H (E = Ge, Si) Bond Activations: Steric Influences on Intramolecular MoH...E Interactions
• Authors of publication: Akihiro Shinohara; Jennifer McBee; T. Don Tilley
• Journal of publication: Inorganic Chemistry
• Year of publication: 2009
• Journal volume: 48
• Pages of publication: 8081 - 8083
• a: 8.7018 ± 0.0008 Å
• b: 17.3143 ± 0.0015 Å
• c: 16.3785 ± 0.0014 Å
• α: 90°
• β: 102.312 ± 0.001°
• γ: 90°
• Cell volume: 2410.9 ± 0.4 ų
• Cell temperature: 153 ± 2 K
• Ambient diffraction temperature: 153 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0335
• Residual factor for significantly intense reflections: 0.0271
• Weighted residual factors for significantly intense reflections: 0.0716
• Weighted residual factors for all reflections included in the refinement: 0.0733
• Goodness-of-fit parameter for all reflections included in the refinement: 0.986
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No