Information card for entry 4303177

Structure parameters

• Formula: C20 H43 Br4 N3 O2 Re
• Calculated formula: C19.532 H41.9938 Br4 N2.9298 O1.9532 Re
• Title of publication: Synthesis and Reactivity of the 17 e-Complex [ReIIBr4(CO)2]2-: A Convenient Entry into Rhenium(II) Chemistry
• Authors of publication: Fabio Zobi; Lukas Kromer; Bernhard Spingler; Roger Alberto
• Journal of publication: Inorganic Chemistry
• Year of publication: 2009
• Journal volume: 48
• Pages of publication: 8965 - 8970
• a: 8.9079 ± 0.0001 Å
• b: 13.8634 ± 0.0002 Å
• c: 23.8045 ± 0.0003 Å
• α: 90°
• β: 95.309 ± 0.0012°
• γ: 90°
• Cell volume: 2927.1 ± 0.07 ų
• Cell temperature: 183 ± 2 K
• Ambient diffraction temperature: 183 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.059
• Residual factor for significantly intense reflections: 0.047
• Weighted residual factors for significantly intense reflections: 0.1236
• Weighted residual factors for all reflections included in the refinement: 0.1274
• Goodness-of-fit parameter for all reflections included in the refinement: 1.303
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No