Crystallography Open Database

Information card for entry 4303297

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Coordinates	4303297.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C35 H45 F3 N2 O S Sn
Calculated formula	C35 H45 F3 N2 O S Sn
SMILES	[Sn]1(OC(C(F)(F)F)c2sccc2)[N](c2c(cccc2C(C)C)C(C)C)=C(C)C=C(N1c1c(cccc1C(C)C)C(C)C)C
Title of publication	Hydrostannylation of Ketones and Alkynes with LSnH [L = HC(CMeNAr)2, Ar = 2,6-iPr2C6H3]
Authors of publication	Anukul Jana; Herbert W. Roesky; Carola Schulzke
Journal of publication	Inorganic Chemistry
Year of publication	2009
Journal volume	48
Pages of publication	9543 - 9548
a	8.8197 ± 0.0018 Å
b	12.061 ± 0.002 Å
c	16.556 ± 0.003 Å
α	81.07 ± 0.03°
β	77.65 ± 0.03°
γ	87.01 ± 0.03°
Cell volume	1699.2 ± 0.6 Å³
Cell temperature	133 ± 2 K
Ambient diffraction temperature	133 ± 2 K
Number of distinct elements	7
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0595
Residual factor for significantly intense reflections	0.0488
Weighted residual factors for significantly intense reflections	0.1348
Weighted residual factors for all reflections included in the refinement	0.1401
Goodness-of-fit parameter for all reflections included in the refinement	1.044
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

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