Information card for entry 4303304

Structure parameters

• Formula: C14 H14 Mo2 S6
• Calculated formula: C14 H14 Mo2 S6
• Title of publication: Sequential Construction of One, Two, or Three Dithiolene Ligands from Alkynes and Sulfur in Dinuclear Cyclopentadienyl Molybdenum Complexes
• Authors of publication: Harry Adams; Matthew N. Bancroft; Michael J. Morris; Andrea E. Riddiough
• Journal of publication: Inorganic Chemistry
• Year of publication: 2009
• Journal volume: 48
• Pages of publication: 9557 - 9566
• a: 7.9933 ± 0.0009 Å
• b: 23.34 ± 0.003 Å
• c: 14.4095 ± 0.0017 Å
• α: 90°
• β: 100.233 ± 0.002°
• γ: 90°
• Cell volume: 2645.5 ± 0.5 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 4
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0548
• Residual factor for significantly intense reflections: 0.0434
• Weighted residual factors for significantly intense reflections: 0.1006
• Weighted residual factors for all reflections included in the refinement: 0.106
• Goodness-of-fit parameter for all reflections included in the refinement: 1.041
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No