Information card for entry 4303342

Structure parameters

• Chemical name: sodium 15-crown-5 trisulfur trintride
• Formula: C10 H20 N3 Na O5 S3
• Calculated formula: C10 H20 N3 Na O5 S3
• Title of publication: Electrochemical and Chemical Reduction of Disulfur Dinitride: Formation of [S4N4]-., EPR Spectroscopic Characterization of the [S2N2H]. Radical, and X-ray Structure of [Na(15-crown-5)][S3N3]
• Authors of publication: Tracey L. Roemmele; Jari Konu; René T. Boeré; Tristram Chivers
• Journal of publication: Inorganic Chemistry
• Year of publication: 2009
• Journal volume: 48
• Pages of publication: 9454 - 9462
• a: 16.158 ± 0.003 Å
• b: 14.383 ± 0.003 Å
• c: 7.3713 ± 0.0015 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 1713.1 ± 0.6 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 6
• Space group number: 62
• Hermann-Mauguin space group symbol: P n m a
• Hall space group symbol: -P 2ac 2n
• Residual factor for all reflections: 0.0952
• Residual factor for significantly intense reflections: 0.0546
• Weighted residual factors for significantly intense reflections: 0.1267
• Weighted residual factors for all reflections included in the refinement: 0.1479
• Goodness-of-fit parameter for all reflections included in the refinement: 1.032
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No