Information card for entry 4303442

Structure parameters

• Formula: C18 H46 Ge33 N8 O75
• Calculated formula: C18 H46 Ge33 N8 O75
• Title of publication: Open-Framework Germanate Built from the Hexagonal Packing of Rigid Cylinders
• Authors of publication: Charlotte Bonneau; Junliang Sun; Rebeca Sanchez-Smith; Bing Guo; Daliang Zhang; Andrew Kentaro Inge; Mattias Edén; Xiaodong Zou
• Journal of publication: Inorganic Chemistry
• Year of publication: 2009
• Journal volume: 48
• Pages of publication: 9962 - 9964
• a: 49.257 ± 0.01 Å
• b: 28.439 ± 0.006 Å
• c: 14.866 ± 0.003 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 20825 ± 7 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 5
• Space group number: 72
• Hermann-Mauguin space group symbol: I b a m
• Hall space group symbol: -I 2 2c
• Residual factor for all reflections: 0.1217
• Residual factor for significantly intense reflections: 0.0749
• Weighted residual factors for significantly intense reflections: 0.1892
• Weighted residual factors for all reflections included in the refinement: 0.2054
• Goodness-of-fit parameter for all reflections included in the refinement: 0.943
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 1.03 Å
• Diffraction radiation type: synchrotron
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No