Information card for entry 4303495

Structure parameters

• Formula: C67 H78 O5 Si
• Calculated formula: C67 H78 O5 Si
• Title of publication: Facile Synthesis of Bismuth(III) and Antimony(III) Complexes Supported by Silylated Calix[5]arenes.
• Authors of publication: Daniel Mendoza-Espinosa; Tracy A. Hanna
• Journal of publication: Inorganic Chemistry
• Year of publication: 2009
• Journal volume: 48
• Pages of publication: 10312 - 10325
• a: 10.98 ± 0.003 Å
• b: 17.101 ± 0.005 Å
• c: 18.085 ± 0.005 Å
• α: 100.073 ± 0.006°
• β: 107.479 ± 0.005°
• γ: 101.844 ± 0.005°
• Cell volume: 3066.6 ± 1.5 ų
• Cell temperature: 213 ± 2 K
• Ambient diffraction temperature: 213 ± 2 K
• Number of distinct elements: 4
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0823
• Residual factor for significantly intense reflections: 0.0528
• Weighted residual factors for significantly intense reflections: 0.1371
• Weighted residual factors for all reflections included in the refinement: 0.1498
• Goodness-of-fit parameter for all reflections included in the refinement: 0.979
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No