Information card for entry 4303497

Structure parameters

• Formula: C61 H81 O7 Sb Si
• Calculated formula: C61 H77 O7 Sb Si
• Title of publication: Facile Synthesis of Bismuth(III) and Antimony(III) Complexes Supported by Silylated Calix[5]arenes.
• Authors of publication: Daniel Mendoza-Espinosa; Tracy A. Hanna
• Journal of publication: Inorganic Chemistry
• Year of publication: 2009
• Journal volume: 48
• Pages of publication: 10312 - 10325
• a: 27.843 ± 0.005 Å
• b: 15.306 ± 0.003 Å
• c: 13.221 ± 0.002 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 5634.3 ± 1.7 ų
• Cell temperature: 218 ± 2 K
• Ambient diffraction temperature: 218 ± 2 K
• Number of distinct elements: 5
• Space group number: 33
• Hermann-Mauguin space group symbol: P n a 21
• Hall space group symbol: P 2c -2n
• Residual factor for all reflections: 0.1047
• Residual factor for significantly intense reflections: 0.0574
• Weighted residual factors for significantly intense reflections: 0.1198
• Weighted residual factors for all reflections included in the refinement: 0.1427
• Goodness-of-fit parameter for all reflections included in the refinement: 0.91
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No