Information card for entry 4303500

Structure parameters

• Formula: C66 H87 Bi O7 Si
• Calculated formula: C66 H87 Bi O7 Si
• Title of publication: Facile Synthesis of Bismuth(III) and Antimony(III) Complexes Supported by Silylated Calix[5]arenes.
• Authors of publication: Daniel Mendoza-Espinosa; Tracy A. Hanna
• Journal of publication: Inorganic Chemistry
• Year of publication: 2009
• Journal volume: 48
• Pages of publication: 10312 - 10325
• a: 13.033 ± 0.004 Å
• b: 15.05 ± 0.005 Å
• c: 18.679 ± 0.006 Å
• α: 66.401 ± 0.005°
• β: 75.309 ± 0.006°
• γ: 67.587 ± 0.005°
• Cell volume: 3081.7 ± 1.7 ų
• Cell temperature: 223 ± 2 K
• Ambient diffraction temperature: 223 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0688
• Residual factor for significantly intense reflections: 0.0474
• Weighted residual factors for significantly intense reflections: 0.1079
• Weighted residual factors for all reflections included in the refinement: 0.1211
• Goodness-of-fit parameter for all reflections included in the refinement: 0.979
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No