Information card for entry 4303503

Structure parameters

• Formula: C72 H97 O8 Sb Si
• Calculated formula: C68 H87 O6 Sb Si
• SMILES: [Sb]1(Oc2c3Cc4cc(cc(Cc5cc(cc6Cc7c(O[Si](Oc56)(C)C)c(cc(c7)C(C)(C)C)Cc5cc(cc(Cc2cc(c3)C(C)(C)C)c5O1)C(C)(C)C)C(C)(C)C)c4OCc1ccccc1)C(C)(C)C)OC(C)(C)C
• Title of publication: Facile Synthesis of Bismuth(III) and Antimony(III) Complexes Supported by Silylated Calix[5]arenes.
• Authors of publication: Daniel Mendoza-Espinosa; Tracy A. Hanna
• Journal of publication: Inorganic Chemistry
• Year of publication: 2009
• Journal volume: 48
• Pages of publication: 10312 - 10325
• a: 31.122 ± 0.003 Å
• b: 31.122 ± 0.003 Å
• c: 14.5433 ± 0.0018 Å
• α: 90°
• β: 90°
• γ: 120°
• Cell volume: 12199 ± 2 ų
• Cell temperature: 223 ± 2 K
• Ambient diffraction temperature: 223 ± 2 K
• Number of distinct elements: 5
• Space group number: 147
• Hermann-Mauguin space group symbol: P -3
• Hall space group symbol: -P 3
• Residual factor for all reflections: 0.0753
• Residual factor for significantly intense reflections: 0.0488
• Weighted residual factors for significantly intense reflections: 0.1311
• Weighted residual factors for all reflections included in the refinement: 0.1432
• Goodness-of-fit parameter for all reflections included in the refinement: 0.969
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No