Information card for entry 4303573

Structure parameters

• Chemical name: (1,2-Bis(dicyclohexylphosphino)ethane)(5,6- dithiolato[1,3]dithiol-2-one)Palladium(II)
• Formula: C33 H50 O P2 Pd S4
• Calculated formula: C33 H50 O P2 Pd S4
• Title of publication: Synthesis, Structures, and Properties of 1,2,4,5-Benzenetetrathiolate Linked Group 10 Metal Complexes
• Authors of publication: Kuppuswamy Arumugam; Mohamed C. Shaw; P. Chandrasekaran; Dino Villagrán; Thomas G. Gray; Joel T. Mague; James P. Donahue
• Journal of publication: Inorganic Chemistry
• Year of publication: 2009
• Journal volume: 48
• Pages of publication: 10591 - 10607
• a: 12.0385 ± 0.0019 Å
• b: 17.43 ± 0.003 Å
• c: 16.389 ± 0.003 Å
• α: 90°
• β: 101.769 ± 0.002°
• γ: 90°
• Cell volume: 3366.6 ± 1 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.1044
• Residual factor for significantly intense reflections: 0.0673
• Weighted residual factors for significantly intense reflections: 0.1512
• Weighted residual factors for all reflections included in the refinement: 0.172
• Goodness-of-fit parameter for all reflections included in the refinement: 1.017
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No