Information card for entry 4303581

Structure parameters

• Chemical name: Di-n-butyltin(μ-1,2,4,5-tetrathiolatobenzene)(1,2-bis(di cyclohexylphosphino)ethane)nickel(II) 1,2-dichloroethane hemisolvate
• Formula: C41 H70 Cl Ni P2 S4 Sn
• Calculated formula: C41 H70 Cl Ni P2 S4 Sn
• Title of publication: Synthesis, Structures, and Properties of 1,2,4,5-Benzenetetrathiolate Linked Group 10 Metal Complexes
• Authors of publication: Kuppuswamy Arumugam; Mohamed C. Shaw; P. Chandrasekaran; Dino Villagrán; Thomas G. Gray; Joel T. Mague; James P. Donahue
• Journal of publication: Inorganic Chemistry
• Year of publication: 2009
• Journal volume: 48
• Pages of publication: 10591 - 10607
• a: 38.367 ± 0.003 Å
• b: 10.3214 ± 0.0009 Å
• c: 48.842 ± 0.004 Å
• α: 90°
• β: 97.497 ± 0.003°
• γ: 90°
• Cell volume: 19176 ± 3 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.1094
• Residual factor for significantly intense reflections: 0.0806
• Weighted residual factors for significantly intense reflections: 0.1687
• Weighted residual factors for all reflections included in the refinement: 0.1795
• Goodness-of-fit parameter for all reflections included in the refinement: 1.086
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No