Information card for entry 4303724

Structure parameters

• Formula: C144 H240 Cl8 N40 O44 Pd6
• Calculated formula: C24 H40 Cl1.33333 N6.66667 O7.33333 Pd
• Title of publication: Self-Assembly of a Pd6-Molecular Double-Square and a Cu3-Trigonalbipyramidal Cage via a New Tripodal Flexible Ligand
• Authors of publication: Arun Kumar Bar; Rajesh Chakrabarty; Partha Sarathi Mukherjee
• Journal of publication: Inorganic Chemistry
• Year of publication: 2009
• Journal volume: 48
• Pages of publication: 10880 - 10882
• a: 16.057 ± 0.003 Å
• b: 18.914 ± 0.004 Å
• c: 22.57 ± 0.005 Å
• α: 105.75 ± 0.03°
• β: 101.71 ± 0.03°
• γ: 93.9 ± 0.03°
• Cell volume: 6405 ± 3 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1046
• Residual factor for significantly intense reflections: 0.0982
• Weighted residual factors for significantly intense reflections: 0.3021
• Weighted residual factors for all reflections included in the refinement: 0.3147
• Goodness-of-fit parameter for all reflections included in the refinement: 1.435
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No