Information card for entry 4303732

Structure parameters

• Formula: C36 H84 Ce2 Cl2 N16 Si8
• Calculated formula: C36 H84 Ce2 Cl2 N16 Si8
• Title of publication: Varied Reactions of [M(L)]3 with HgCl2, FeBr2, CeCl3, AgOTf; Ligand Transfer, Nucleophilic Attack with Recombination and/or Fragmentation [M = Li or Na; L = N(SiMe3){C(H)N}3SiMe3]
• Authors of publication: W. Marco Boesveld; Peter B. Hitchcock; Michael F. Lappert
• Journal of publication: Inorganic Chemistry
• Year of publication: 2009
• Journal volume: 48
• Pages of publication: 11444 - 11450
• a: 10.941 ± 0.002 Å
• b: 27.269 ± 0.004 Å
• c: 10.953 ± 0.002 Å
• α: 90°
• β: 94.78 ± 0.02°
• γ: 90°
• Cell volume: 3256.5 ± 1 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0992
• Residual factor for significantly intense reflections: 0.072
• Weighted residual factors for all reflections: 0.2183
• Weighted residual factors for all reflections included in the refinement: 0.1686
• Goodness-of-fit parameter for all reflections: 1.026
• Goodness-of-fit parameter for all reflections included in the refinement: 1.039
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No