Information card for entry 4303745

Structure parameters

• Common name: [Xanthdim][MgN(SiMe3)2(THF)]2.(C6H6)2.5
• Formula: C96 H135 Mg2 N6 O3 Si4
• Calculated formula: C96 H135 Mg2 N6 O3 Si4
• Title of publication: Peculiar Binding Modes of a Ligand with Two Adjacent β-Diiminato Binding Sites in Alkali and Alkaline-Earth Metal Chemistry
• Authors of publication: Dirk F.-J. Piesik; Peter Haack; Sjoerd Harder; Christian Limberg
• Journal of publication: Inorganic Chemistry
• Year of publication: 2009
• Journal volume: 48
• Pages of publication: 11259 - 11264
• a: 18.326 ± 0.002 Å
• b: 27.314 ± 0.003 Å
• c: 21.13 ± 0.002 Å
• α: 90°
• β: 115.644 ± 0.006°
• γ: 90°
• Cell volume: 9535 ± 1.8 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.1145
• Residual factor for significantly intense reflections: 0.0658
• Weighted residual factors for significantly intense reflections: 0.1585
• Weighted residual factors for all reflections included in the refinement: 0.1879
• Goodness-of-fit parameter for all reflections included in the refinement: 1.028
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No