Information card for entry 4303762

Structure parameters

• Formula: C32.47 H47.93 Cl0.93 Mo N2 O4
• Calculated formula: C32.462 H47.924 Cl0.924 Mo N2 O4
• Title of publication: An Efficient Method for the Preparation of Oxo Molybdenum Salalen Complexes and Their Unusual Use as Hydrosilylation Catalysts
• Authors of publication: Jeanette E. Ziegler; Guodong Du; Philip E. Fanwick; Mahdi M. Abu-Omar
• Journal of publication: Inorganic Chemistry
• Year of publication: 2009
• Journal volume: 48
• Pages of publication: 11290 - 11296
• a: 14.569 ± 0.003 Å
• b: 15.011 ± 0.006 Å
• c: 18.323 ± 0.005 Å
• α: 72.878 ± 0.013°
• β: 88.824 ± 0.007°
• γ: 72.504 ± 0.011°
• Cell volume: 3642 ± 2 ų
• Cell temperature: 150 K
• Ambient diffraction temperature: 150 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.089
• Residual factor for significantly intense reflections: 0.057
• Weighted residual factors for significantly intense reflections: 0.144
• Weighted residual factors for all reflections included in the refinement: 0.156
• Goodness-of-fit parameter for all reflections included in the refinement: 1.021
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MO-Kα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No