Information card for entry 4303768

Structure parameters

• Formula: C38 H33 Al B F15 Li O2 P
• Calculated formula: C38 H33 Al B F15 Li O2 P
• SMILES: Fc1c(c(F)c(F)c(F)c1F)[Al](c1c(F)c(F)c(F)c(F)c1F)(c1c(F)c(F)c(F)c(F)c1F)[P]([BH]1[H][Li]([H]1)([O](CC)CC)[O](CC)CC)(c1ccccc1)c1ccccc1
• Title of publication: Synthesis, Structure, and Stability of Adducts between Phosphide and Amide Anions and the Lewis Acids Borane, Tris(pentafluorophenyl)borane, and Tris(pentafluorophenyl)alane
• Authors of publication: Anna-Marie Fuller; Andrew J. Mountford; Matthew L. Scott; Simon J. Coles; Peter N. Horton; David L. Hughes; Michael B. Hursthouse; Simon J. Lancaster
• Journal of publication: Inorganic Chemistry
• Year of publication: 2009
• Journal volume: 48
• Pages of publication: 11474 - 11482
• a: 12.277 ± 0.002 Å
• b: 12.334 ± 0.002 Å
• c: 14.628 ± 0.003 Å
• α: 84.969 ± 0.012°
• β: 71.244 ± 0.013°
• γ: 73.58 ± 0.014°
• Cell volume: 2011.9 ± 0.7 ų
• Cell temperature: 120 ± 2 K
• Ambient diffraction temperature: 120 ± 2 K
• Number of distinct elements: 8
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0684
• Residual factor for significantly intense reflections: 0.0573
• Weighted residual factors for significantly intense reflections: 0.1422
• Weighted residual factors for all reflections included in the refinement: 0.1501
• Goodness-of-fit parameter for all reflections included in the refinement: 1.13
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No