Information card for entry 4303846

Structure parameters

• Formula: C39 H57 I N4 Se U
• Calculated formula: C32 I1.021 N4 Se0.979 U
• Title of publication: Oxidative Addition to U(V)-U(V) Dimers: Facile Routes to Uranium(VI) Bis(imido) Complexes
• Authors of publication: Liam P. Spencer; Ping Yang; Brian L. Scott; Enrique R. Batista; James M. Boncella
• Journal of publication: Inorganic Chemistry
• Year of publication: 2009
• Journal volume: 48
• Pages of publication: 11615 - 11623
• a: 13.928 ± 0.003 Å
• b: 14.961 ± 0.003 Å
• c: 20.327 ± 0.004 Å
• α: 90°
• β: 96.152 ± 0.002°
• γ: 90°
• Cell volume: 4211.3 ± 1.5 ų
• Cell temperature: 120 ± 1 K
• Ambient diffraction temperature: 120 ± 1 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0709
• Residual factor for significantly intense reflections: 0.0464
• Weighted residual factors for significantly intense reflections: 0.1166
• Weighted residual factors for all reflections included in the refinement: 0.1252
• Goodness-of-fit parameter for all reflections included in the refinement: 1.009
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No