Information card for entry 4303916

Structure parameters

• Formula: C138 H115 B8 F32 N42 Ni4 O0.5
• Calculated formula: C138 H114 B8 F32 N42 Ni4 O0.5
• Title of publication: Cubes, Squares, and Books: A Simple Transition Metal/Bridging Ligand Combination Can Lead to a Surprising Range of Structural Types with the Same Metal/Ligand Proportions
• Authors of publication: Adel M. Najar; Ian S. Tidmarsh; Harry Adams; Michael D. Ward
• Journal of publication: Inorganic Chemistry
• Year of publication: 2009
• Journal volume: 48
• Pages of publication: 11871 - 11881
• a: 21.3802 ± 0.0015 Å
• b: 19.4021 ± 0.0015 Å
• c: 37.083 ± 0.003 Å
• α: 90°
• β: 103.357 ± 0.003°
• γ: 90°
• Cell volume: 14967 ± 2 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 7
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.1596
• Residual factor for significantly intense reflections: 0.1346
• Weighted residual factors for significantly intense reflections: 0.3608
• Weighted residual factors for all reflections included in the refinement: 0.3765
• Goodness-of-fit parameter for all reflections included in the refinement: 1.025
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No