Crystallography Open Database

Information card for entry 4304349

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Structure parameters

Formula	C34 H41 Br Cl2 N O P
Calculated formula	C34 H41 Br Cl2 N O P
SMILES	[Br-].ClCCl.[P+](c1ccccc1)(c1ccccc1)(c1ccccc1)C=C(Nc1c(C(C)C)cccc1C(C)C)C.O
Title of publication	Nickel(II) Complexes Containing Bidentate Amido Phosphine Ligands Derived from α-Iminophosphorus Ylides: Synthesis and Structural Characterization
Authors of publication	Pei-Ying Lee; Lan-Chang Liang
Journal of publication	Inorganic Chemistry
Year of publication	2008
Journal volume	47
Pages of publication	749 - 758
a	9.8565 ± 0.0003 Å
b	11.3286 ± 0.0003 Å
c	15.5802 ± 0.0005 Å
α	79.6019 ± 0.0011°
β	83.6492 ± 0.0011°
γ	88.124 ± 0.002°
Cell volume	1700.47 ± 0.09 Å³
Cell temperature	298 K
Number of distinct elements	7
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.1519
Residual factor for significantly intense reflections	0.1146
Weighted residual factors for significantly intense reflections	0.3181
Weighted residual factors for all reflections included in the refinement	0.3463
Goodness-of-fit parameter for all reflections included in the refinement	2.232
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

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