Information card for entry 4304438

Structure parameters

• Formula: C21.5 H26 Cl6.5 N3 O2 P Ru
• Calculated formula: C21.5 H26 Cl6.5 N3 O2 P Ru
• Title of publication: Insertion of CO2, Ketones, and Aldehydes into the C-Li Bond of 1,3,5-Triaza-7-phosphaadamantan-6-yllithium
• Authors of publication: Gene W. Wong; Wei-Chih Lee; Brian J. Frost
• Journal of publication: Inorganic Chemistry
• Year of publication: 2008
• Journal volume: 47
• Pages of publication: 612 - 620
• a: 13.1047 ± 0.0004 Å
• b: 14.6644 ± 0.0004 Å
• c: 15.722 ± 0.0005 Å
• α: 66.146 ± 0.001°
• β: 87.292 ± 0.001°
• γ: 82.381 ± 0.001°
• Cell volume: 2738.79 ± 0.14 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0909
• Residual factor for significantly intense reflections: 0.0552
• Weighted residual factors for significantly intense reflections: 0.1341
• Weighted residual factors for all reflections included in the refinement: 0.1491
• Goodness-of-fit parameter for all reflections included in the refinement: 1.093
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No