Information card for entry 4305128

Structure parameters

• Formula: C37 H43 N P Rh
• Calculated formula: C37 H43 N P Rh
• Title of publication: Cyclic (Amino)[bis(ylide)]carbene as an Anionic Bidentate Ligand for Transition-Metal Complexes
• Authors of publication: Matthew Asay; Bruno Donnadieu; Antoine Baceiredo; Michele Soleilhavoup; Guy Bertrand
• Journal of publication: Inorganic Chemistry
• Year of publication: 2008
• Journal volume: 47
• Pages of publication: 3949 - 3951
• a: 10.0764 ± 0.0009 Å
• b: 19.8136 ± 0.0019 Å
• c: 15.5223 ± 0.0014 Å
• α: 90°
• β: 93.112 ± 0.005°
• γ: 90°
• Cell volume: 3094.5 ± 0.5 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0374
• Residual factor for significantly intense reflections: 0.0278
• Weighted residual factors for significantly intense reflections: 0.0673
• Weighted residual factors for all reflections included in the refinement: 0.0719
• Goodness-of-fit parameter for all reflections included in the refinement: 1.024
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No