Information card for entry 4305729

Structure parameters

• Formula: C19 H21 N2 O2 Rh
• Calculated formula: C19 H21 N2 O2 Rh
• SMILES: [Rh]12([n]3c(C=[N]1c1c(cccc1C)C)cccc3)OC(=CC(=[O]2)C)C
• Title of publication: Synthesis, Characterization, and Reactivity of Rhodium(I) Acetylacetonato Complexes Containing Pyridinecarboxaldimine Ligands
• Authors of publication: Diane A. Kanas; Stephen J. Geier; Christopher M. Vogels; Andreas Decken; Stephen A. Westcott
• Journal of publication: Inorganic Chemistry
• Year of publication: 2008
• Journal volume: 47
• Pages of publication: 8727 - 8735
• a: 9.442 ± 0.006 Å
• b: 7.753 ± 0.005 Å
• c: 24.08 ± 0.016 Å
• α: 90°
• β: 90.896 ± 0.011°
• γ: 90°
• Cell volume: 1763 ± 2 ų
• Cell temperature: 173 ± 1 K
• Ambient diffraction temperature: 173 ± 1 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0517
• Residual factor for significantly intense reflections: 0.0426
• Weighted residual factors for significantly intense reflections: 0.1153
• Weighted residual factors for all reflections included in the refinement: 0.1172
• Goodness-of-fit parameter for all reflections included in the refinement: 1.023
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No