Information card for entry 4306109

Structure parameters

• Formula: C28 H57 Cl Fe N4 P2 Si2
• Calculated formula: C28 H57 Cl Fe N4 P2 Si2
• Title of publication: Influence of the Metal Orbital Occupancy and Principal Quantum Number on Organoazide (RN3) Conversion to Transition-Metal Imide Complexes
• Authors of publication: Amy N. Walstrom; Benjamin C. Fullmer; Hongjun Fan; Maren Pink; Drew T. Buschhorn; Kenneth G. Caulton
• Journal of publication: Inorganic Chemistry
• Year of publication: 2008
• Journal volume: 47
• Pages of publication: 9002 - 9009
• a: 10.3791 ± 0.0011 Å
• b: 19.769 ± 0.002 Å
• c: 20.381 ± 0.002 Å
• α: 62.619 ± 0.002°
• β: 79.132 ± 0.003°
• γ: 76.79 ± 0.003°
• Cell volume: 3598.2 ± 0.6 ų
• Cell temperature: 130 ± 2 K
• Ambient diffraction temperature: 130 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0553
• Residual factor for significantly intense reflections: 0.0363
• Weighted residual factors for significantly intense reflections: 0.0845
• Weighted residual factors for all reflections included in the refinement: 0.0955
• Goodness-of-fit parameter for all reflections included in the refinement: 1.006
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No