Information card for entry 4306597

Structure parameters

• Formula: C96 H80 Cu2 N24 O14 P4 Pt2
• Calculated formula: C96 H80 Cu2 N24 O14 P4 Pt2
• Title of publication: PtII-Promoted [2 + 3] Cycloaddition of Azide to Cyanopyridines: Convenient Tool toward Heterometallic Structures
• Authors of publication: Suman Mukhopadhyay; Bhaswati Ghosh Mukhopadhyay; M. Fátima C. Guedes da Silva; Jamal Lasri; M. Adília Januário Charmier; Armando J. L. Pombeiro
• Journal of publication: Inorganic Chemistry
• Year of publication: 2008
• Journal volume: 47
• Pages of publication: 11334 - 11341
• a: 13.4734 ± 0.0003 Å
• b: 14.0405 ± 0.0002 Å
• c: 15.924 ± 0.0003 Å
• α: 83.711 ± 0.0011°
• β: 71.975 ± 0.0013°
• γ: 75.227 ± 0.001°
• Cell volume: 2768.32 ± 0.09 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0476
• Residual factor for significantly intense reflections: 0.037
• Weighted residual factors for significantly intense reflections: 0.0889
• Weighted residual factors for all reflections included in the refinement: 0.0926
• Goodness-of-fit parameter for all reflections included in the refinement: 1.081
• Diffraction radiation wavelength: 0.71069 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No