Information card for entry 4306649

Structure parameters

• Formula: C64 H98 Co Na O7
• Calculated formula: C64 H78 Co Na O7
• Title of publication: One- and Two-Electron Reduced 1,2-Diketone Ligands in [ZnII(L.)2(Et2O)], [CoII(L.)2(Et2O)], and Na2(Et2O)4[CoII(LRed)2]
• Authors of publication: Geoffrey H. Spikes; Carsten Milsmann; Eckhard Bill; Thomas Weyhermüller; Karl Wieghardt
• Journal of publication: Inorganic Chemistry
• Year of publication: 2008
• Journal volume: 47
• Pages of publication: 11745 - 11754
• a: 10.235 ± 0.0008 Å
• b: 12.7244 ± 0.0013 Å
• c: 13.19 ± 0.0013 Å
• α: 71.472 ± 0.004°
• β: 74.95 ± 0.005°
• γ: 88.42 ± 0.005°
• Cell volume: 1570.1 ± 0.3 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0928
• Residual factor for significantly intense reflections: 0.0607
• Weighted residual factors for significantly intense reflections: 0.1373
• Weighted residual factors for all reflections included in the refinement: 0.1565
• Goodness-of-fit parameter for all reflections included in the refinement: 1.029
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No