Information card for entry 4306683

Structure parameters

• Chemical name: 2,3-bis-(trimethylsilyl)-4,4-bis-(trimethylsilyl)-cyclo-2-phospha-4-sila-2,3- diazenium tetrachlorogallate
• Formula: C12 H36 Cl4 Ga N2 P Si5
• Calculated formula: C12 H36 Cl4 Ga N2 P Si5
• Title of publication: GaCl3-Assisted Cyclization Reactions in Hypersilyl(trimethylsilyl)aminodichlorophosphine
• Authors of publication: Alexander Villinger; Andrea Westenkirchner; Ronald Wustrack; Axel Schulz
• Journal of publication: Inorganic Chemistry
• Year of publication: 2008
• Journal volume: 47
• Pages of publication: 9140 - 9142
• a: 16.101 ± 0.003 Å
• b: 12.561 ± 0.003 Å
• c: 18.617 ± 0.007 Å
• α: 90°
• β: 125.069 ± 0.018°
• γ: 90°
• Cell volume: 3081.7 ± 1.6 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0443
• Residual factor for significantly intense reflections: 0.0266
• Weighted residual factors for significantly intense reflections: 0.0638
• Weighted residual factors for all reflections included in the refinement: 0.0705
• Goodness-of-fit parameter for all reflections included in the refinement: 1.032
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No