Information card for entry 4306740

Structure parameters

• Formula: C58 H53 N20 Ni5 O30.5
• Calculated formula: C58 H53 N20 Ni5 O30.5
• Title of publication: Unusual Structural Types in Nickel Cluster Chemistry from the Use of Pyridyl Oximes: Ni5, Ni12Na2, and Ni14 Clusters
• Authors of publication: Theocharis C. Stamatatos; Albert Escuer; Khalil A. Abboud; Catherine P. Raptopoulou; Spyros P. Perlepes; George Christou
• Journal of publication: Inorganic Chemistry
• Year of publication: 2008
• Journal volume: 47
• Pages of publication: 11825 - 11838
• a: 17.68 ± 0.009 Å
• b: 14.989 ± 0.009 Å
• c: 15.584 ± 0.008 Å
• α: 98.269 ± 0.017°
• β: 96.167 ± 0.016°
• γ: 106.223 ± 0.016°
• Cell volume: 3877 ± 4 ų
• Cell temperature: 298 K
• Ambient diffraction temperature: 298 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0797
• Residual factor for significantly intense reflections: 0.0564
• Weighted residual factors for significantly intense reflections: 0.1498
• Weighted residual factors for all reflections included in the refinement: 0.1678
• Goodness-of-fit parameter for all reflections included in the refinement: 1.075
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No